Explain the working and components of gas chromatograph with help of a neat, labeled, schematic block diagram.
[6 marks]Write a note on ISO 9000.
[4 marks]Explain the principle of NMR spectroscopy.
[4 marks]Discuss retention mechanism, instrumentation and applications of HPLC.
[6 marks]Write the steps involved in analysis of drugs using HPTLC method.
[4 marks]What is ICH guidelines? Enlist types of guidelines. Enlist quality guidelines.
[4 marks]What are the reference and indicator electrodes used in potentiometric titrations? Discuss the methods of detecting end point in potentiometric titrations.
[6 marks]What is electrophoresis? Classify electrophoresis. Write applications.
[4 marks]Explain the theory of Gel Filtration Chromatography. Write applications.
[4 marks]What is conductometric titration? Explain them with suitable examples.
[6 marks]Explain the theory of polarography involving Ilkovic equation.
[4 marks]What are different methods of Thermal analysis? Explain DSC in detail.
[4 marks]State and derive Lambert-Beer’s law. What is deviation from Beer’s law, Enlist various types of deviation.
[6 marks]Explain the principle of Atomic absorption Spectroscopy. Give its applications.
[4 marks]Explain: Chromatography. Give a suitable classification of various chromatographic techniques with examples Q. 6 (a) Write a note on radiation sources and detectors used in IR spectroscopy. Explain Fingerprint Region.
[6 marks]Explain principle and pharmaceutical applications of Mass Spectrometry.
[4 marks]Explain theory of X-ray diffraction. Write applications of XRD.
[4 marks]What is quenching? Write types of Quenching with examples. Write pharmaceutical applications of fluorescence spectroscopy.
[6 marks]Explain the principle and instrumentation of polarimeter.
[4 marks]Enlist fuel and oxidants used in Flame photometry. Draw a well-labeled diagram of Flame emission photometer and write function of each component
[4 marks]